6,7-二氢-5H-环戊烷并[b]吡啶的合成Synthesis of 6,7-dihydro-5H- cyclopentano[b] pyridine
宫平,赵燕芳,余德胜
GONG Ping; ZHAO Yan fang; YU De sheng (Department of Pharmaceutics;
摘要(Abstract):
以“一勺烩”方法制备中间体O 烯丙基 环戊酮肟 ,无需分离纯化化合物O 烯丙基羟胺 ,热解反应以氧气代替空气 ,制得 6 ,7 二氢 5H 环戊烷并 [b]吡啶 ,反应总收率为 35 %。
O Allyl cyclopentanone oxime intermediate was prepared by the “one pot” method,and the thermolysis of it in oxygen gave 6,7 dihydro 5 H cyclopentano[b]pyridine, the total yield was 35%.
关键词(KeyWords):
O-烯丙基环戊酮肟;“一勺烩”;6,7-二氢-5H-环戊烷并[b]吡啶;合成
O-allyl cyclopentanone oxime; “one pot” method; 6,7 dihydro 5-H - cyclopentano[b]pyridine; synthesiX
基金项目(Foundation):
作者(Authors):
宫平,赵燕芳,余德胜
GONG Ping; ZHAO Yan fang; YU De sheng (Department of Pharmaceutics;
参考文献(References):
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- O-烯丙基环戊酮肟
- “一勺烩”
- 6,7-二氢-5H-环戊烷并[b]吡啶
- 合成
O-allyl cyclopentanone oxime - “one pot” method
- 6,7 dihydro 5-H - cyclopentano[b]pyridine
- synthesiX